Technical Data Sheet
LOCTITE®290™
December-2013
PRODUCT DESCRIPTION
LOCTITE®290™ provides the following product
characteristics:
Technology Acrylic
Chemical Type Dimethacrylate ester
Appearance (uncured) Green liquidLMS
Fluorescence Positive under UV lightLMS
Components One component -
requires no mixing
Viscosity Low
Cure Anaerobic
Secondary Cure Activator
Application Threadlocking
Strength Medium to High
LOCTITE®290™ is designed for the locking and sealing of
threaded fasteners. Because of its low viscosity and capillary
action, the product wicks between engaged threads and
eliminates the need to disassemble prior to application. The
product cures when confined in the absence of air between
close fitting metal surfaces and prevents loosening and
leakage from shock and vibration. The product can also fill
porosity in welds, castings and powdered metal parts.
Mil-S-46163A
LOCTITE®290™ is tested to the lot requirements of Military
Specification Mil-S-46163A. Note: This is a regional approval.
Please contact your local Technical Service Center for more
information and clarification.
ASTM D5363
Each lot of adhesive produced in North America is tested to
the general requirements defined in paragraphs 5.1.1 and
5.1.2 and to the Detail Requirements defined in section 5.2.
NSF International
Registered to NSF Category P1 for use as a sealant where
there is no possibilty of food contact in and around food
processing areas. Note: This is a regional approval. Please
contact your local Technical Service Center for more
information and clarification.
NSF International
Certified to ANSI/NSF Standard 61 for use in commercial and
residential potable water systems not exceeding 82° C. Note:
This is a regional approval. Please contact your local Technical
Service Center for more information and clarification.
TYPICAL PROPERTIES OF UNCURED MATERIAL
Specific Gravity @ 25 °C 1.08
Flash Point - See SDS
Viscosity, Brookfield - RVT, 25 °C, mPa·s (cP):
Spindle 1, speed 50 rpm, 20 to 55LMS
TYPICAL CURING PERFORMANCE
Cure Speed vs. Substrate
The rate of cure will depend on the substrate used. The graph
below shows the breakaway strength developed with time on
M10 steel nuts and bolts compared to different materials and
tested according to ISO 10964.
% of Full Strength on Steel
Cure Time
100
75
50
25
0
1min 5min10min 30min 1h 3h 6h 24h 72h
Steel
Brass
Zinc dichromate
Stainless steel
Cure Speed vs. Bond Gap
The rate of cure will depend on the bondline gap. Gaps in
threaded fasteners depends on thread type, quality and size.
The following graph shows shear strength developed with time
on steel pins and collars at different controlled gaps and tested
according to ISO 10123.
% of Full Strength on Steel
Cure Time
100
75
50
25
0
1min 5min10min 30min 1h 3h 6h 24h 72h
0.05 mm
0.15 mm
TDS LOCTITE®290™, December-2013
Cure Speed vs. Temperature
The rate of cure will depend on the temperature. The graph
below shows the breakaway strength developed with time at
different temperatures on M10 steel nuts and bolts and tested
according to ISO 10964.
% of Full Strength on Steel
Cure Time
100
75
50
25
0
1min 5min10min 30min 1h 3h 6h 24h 72h
40 °C
22 °C
5 °C
Cure Speed vs. Activator
Where cure speed is unacceptably long, or large gaps are
present, applying activator to the surface will improve cure
speed. The graph below shows the breakaway strength
developed with time on M10 zinc dichromate steel nuts and
bolts using Activator 7471™ and 7649™ and tested according
to ISO 10964.
% of Full Strength on Steel
Cure Time
100
75
50
25
0
1min 5min10min 30min 1h 3h 6h 24h 72h
Activator 7471™
Activator 7649™
No activator
TYPICAL PROPERTIES OF CURED MATERIAL
Physical Properties:
Coefficient of Thermal Expansion,
ISO 11359-2, K-1
80×10-6
Coefficient of Thermal Conductivity, ISO 8302,
W/(m·K)
0.1
Specific Heat, kJ/(kg·K) 0.3
TYPICAL PERFORMANCE OF CURED MATERIAL
Adhesive Properties
After 24 hours @ 22 °C
Breakaway Torque, ISO 10964:
M10 steel nuts and bolts N·m 10
(lb.in.) (90)
Prevail Torque, ISO 10964:
M10 steel nuts and bolts N·m 29
(lb.in.) (260)
Breakloose Torque, ISO 10964, Pre-torqued to 5 N·m:
M10 steel nuts and bolts N·m 30
(lb.in.) (270)
Max. Prevail Torque, ISO 10964, Pre-torqued to 5 N·m:
M10 steel nuts and bolts N·m 40
(lb.in.) (350)
Compressive Shear Strength, ISO 10123:
Steel pins and collars N/mm² ≥5.4LMS
(psi) (≥780)
TYPICAL ENVIRONMENTAL RESISTANCE
Cured for 1 week @ 22 °C
Breakloose Torque, ISO 10964, Pre-torqued to 5 N·m:
M10 zinc phosphate steel nuts and bolts:
Hot Strength
Tested at temperature
% Strength @ 22 °C
Temperature, °C
100
75
50
25
0
0 50 100 150
Heat Aging
Aged at temperature indicated and tested @ 22 °C
% Initial Strength @ 22 °C
Exposure Time, hours
125
100
75
50
25
0
0 1000 2000 3000 4000 5000
100 °C
120 °C
150 °C
Henkel Americas
+860.571.5100
Henkel Europe
+49.89.320800.1800
Henkel Asia Pacific
+86.21.2891.8859
For the most direct access to local sales and technical support visit: www.henkel.com/industrial
TDS LOCTITE®290™, December-2013
Chemical/Solvent Resistance
Aged under conditions indicated and tested @ 22 °C.
% of initial strength
Environment °C 100 h 500 h 1000 h 5000 h
Motor oil (MIL-L-46152) 125 85 85 50 50
Leaded Petrol 22 90 90 90 90
Brake fluid 22 90 90 85 85
Water/glycol 50/50 87 90 90 90 90
Acetone 22 85 85 85 85
Ethanol 22 80 80 80 80
DEF (AdBlue®)22 110 110 135
GENERAL INFORMATION
This product is not recommended for use in pure oxygen
and/or oxygen rich systems and should not be selected as
a sealant for chlorine or other strong oxidizing materials.
For safe handling information on this product, consult the
Safety Data Sheet (SDS).
Where aqueous washing systems are used to clean the
surfaces before bonding, it is important to check for
compatibility of the washing solution with the adhesive. In
some cases these aqueous washes can affect the cure and
performance of the adhesive.
This product is not normally recommended for use on plastics
(particularly thermoplastic materials where stress cracking of
the plastic could result). Users are recommended to confirm
compatibility of the product with such substrates.
Directions for use:
For Pre-assembled Threaded Parts with Thru Holes
1. Prior to assembly, clean all threads (bolt and hole) with a
LOCTITE® cleaning solvent and allow to dry.
2. For Thru Holes, apply several drops of product at screw
and body juncture.
3. Avoid touching the bottle tip to the metal surface.
For Assembly
1. For Blind Holes, apply several drops of the product
down the internal threads to the bottom of the hole
For Porosity Sealing
1. Clean area and apply localized heat to the area to
approximately 121°C.
2. Allow to cool to approximately 85°C and apply the
product.
For Disassembly
1. Remove with standard hand tools.
2. In rare instances where hand tools do not work because
of excessive engagement length, apply localized heat to
nut or bolt to approximately 250 °C. Disassemble while
hot.
For Cleanup
1. Cured product can be removed with a combination of
soaking in a LOCTITE® solvent and mechanical
abrasion such as a wire brush.
Loctite Material SpecificationLMS
LMS dated September-01, 1995. Test reports for each batch
are available for the indicated properties. LMS test reports
include selected QC test parameters considered appropriate to
specifications for customer use. Additionally, comprehensive
controls are in place to assure product quality and
consistency. Special customer specification requirements may
be coordinated through Henkel Quality.
Storage
Store product in the unopened container in a dry location.
Storage information may be indicated on the product container
labeling.
Optimal Storage: 8 °C to 21 °C. Storage below 8 °C or
greater than 28 °C can adversely affect product properties.
Material removed from containers may be contaminated during
use. Do not return product to the original container. Henkel
Corporation cannot assume responsibility for product which
has been contaminated or stored under conditions other than
those previously indicated. If additional information is required,
please contact your local Technical Service Center or
Customer Service Representative.
Conversions
(°C x 1.8) + 32 = °F
kV/mm x 25.4 = V/mil
mm / 25.4 = inches
µm / 25.4 = mil
N x 0.225 = lb
N/mm x 5.71 = lb/in
N/mm² x 145 = psi
MPa x 145 = psi
N·m x 8.851 = lb·in
N·m x 0.738 = lb·ft
N·mm x 0.142 = oz·in
mPa·s = cP
Note:
The information provided in this Technical Data Sheet (TDS) including the
recommendations for use and application of the product are based on our
knowledge and experience of the product as at the date of this TDS. The product
can have a variety of different applications as well as differing application and
working conditions in your environment that are beyond our control. Henkel is,
therefore, not liable for the suitability of our product for the production processes
and conditions in respect of which you use them, as well as the intended
applications and results. We strongly recommend that you carry out your own
prior trials to confirm such suitability of our product.
Any liability in respect of the information in the Technical Data Sheet or any other
written or oral recommendation(s) regarding the concerned product is excluded,
except if otherwise explicitly agreed and except in relation to death or personal
injury caused by our negligence and any liability under any applicable mandatory
product liability law.
In case products are delivered by Henkel Belgium NV, Henkel Electronic
Materials NV, Henkel Nederland BV, Henkel Technologies France SAS and
Henkel France SA please additionally note the following:
In case Henkel would be nevertheless held liable, on whatever legal ground,
Henkel’s liability will in no event exceed the amount of the concerned delivery.
In case products are delivered by Henkel Colombiana, S.A.S. the following
disclaimer is applicable:
The information provided in this Technical Data Sheet (TDS) including the
recommendations for use and application of the product are based on our
knowledge and experience of the product as at the date of this TDS. Henkel is,
therefore, not liable for the suitability of our product for the production processes
and conditions in respect of which you use them, as well as the intended
applications and results. We strongly recommend that you carry out your own
Henkel Americas
+860.571.5100
Henkel Europe
+49.89.320800.1800
Henkel Asia Pacific
+86.21.2891.8859
For the most direct access to local sales and technical support visit: www.henkel.com/industrial
TDS LOCTITE®290™, December-2013
prior trials to confirm such suitability of our product.
Any liability in respect of the information in the Technical Data Sheet or any other
written or oral recommendation(s) regarding the concerned product is excluded,
except if otherwise explicitly agreed and except in relation to death or personal
injury caused by our negligence and any liability under any applicable mandatory
product liability law.
In case products are delivered by Henkel Corporation, Resin Technology
Group, Inc., or Henkel Canada Corporation, the following disclaimer is
applicable:
The data contained herein are furnished for information only and are believed to
be reliable. We cannot assume responsibility for the results obtained by others
over whose methods we have no control. It is the user's responsibility to
determine suitability for the user's purpose of any production methods mentioned
herein and to adopt such precautions as may be advisable for the protection of
property and of persons against any hazards that may be involved in the handling
and use thereof. In light of the foregoing, Henkel Corporation specifically
disclaims all warranties expressed or implied, including warranties of
merchantability or fitness for a particular purpose, arising from sale or use
of Henkel Corporation’s products. Henkel Corporation specifically
disclaims any liability for consequential or incidental damages of any kind,
including lost profits. The discussion herein of various processes or
compositions is not to be interpreted as representation that they are free from
domination of patents owned by others or as a license under any Henkel
Corporation patents that may cover such processes or compositions. We
recommend that each prospective user test his proposed application before
repetitive use, using this data as a guide. This product may be covered by one or
more United States or foreign patents or patent applications.
Trademark usage
Except as otherwise noted, all trademarks in this document are trademarks of
Henkel Corporation in the U.S. and elsewhere. ® denotes a trademark
registered in the U.S. Patent and Trademark Office.
Reference 0.8
Henkel Americas
+860.571.5100
Henkel Europe
+49.89.320800.1800
Henkel Asia Pacific
+86.21.2891.8859
For the most direct access to local sales and technical support visit: www.henkel.com/industrial