DP460NS-1.25OZ - 3M - Datasheet.Live

Scotch-Weld™ Epoxy Adhesives

DP460 Off-White and

DP460NS

Technical Data Sheet January 2019

Product Description 3M™ Scotch-Weld™ Epoxy Adhesives DP460 Off-White and DP460NS

are high performance, two-part epoxy adhesives offering outstanding

shear and peel adhesion, and very high levels of durability.

Features • High shear strength • High peel strength

• 60 minute work life • Non sag (DP460NS)

• Easy mixing

Typical Uncured

Physical

Properties

Note: The following technical information and data should be considered

representative or typical only and should not be used for specification purposes.

Product

3M™ Scotch-Weld™

Epoxy Adhesive

DP460 Off-White

3M™ Scotch-Weld™

Epoxy Adhesive

DP460NS

Viscosity (approx.)

@ 73°F (23°C)

Base

Accelerator

20,000-50,000 cps

8,000-14,000 cps

150,000-275,000 cps

8,000-14,000 cps

Base Resin

Base

Accelerator

epoxy

amine

epoxy

amine

Color

Base

Accelerator

white

amber

white

amber

Net Weight

Base

9.3-9.7

Lbs./Gallon

Accelerator

8.8-9.2

Mix Ratio (B:A)

Volume

2:1

Weight

2:0.96

Work life, 73°F (23°C)

20 g mixed

10 g mixed

5 g mixed

60 minutes

75 minutes

90 minutes

60 minutes

3M™ Scotch-Weld™ Epoxy Adhesives

DP460 Off-White • DP460NS

Typical Cured

Thermal

Properties

Note: The following technical information and data should be considered

representative or typical only and should not be used for specification purposes.

Product

3M™ Scotch-Weld™

Epoxy Adhesive

DP460 Off-White

3M™ Scotch-Weld™

Epoxy Adhesive

DP460NS

Physical

Color

Off-white

Shore D Hardness

75-80

78-84

Thermal

Coefficient of Below Tg

Thermal Expansion Above Tg

(in./in./°C)

59 x 10-6

159 x 10-6

74.44 x 10-6

166 x 10-6

Thermal Conductivity

(btu - ft./ft.2 - hr. - °F) @ 45°C

0.104

Electrical

Dielectric Strength (ASTM D 149)

1100 volts/mil

727 volts/mil

Volume Resistivity (ASTM D 257)

2.4 x 1014 ohm-cm

3.25 x 1015 ohm-cm

Typical Curing

Characteristics

Note: The following technical information and data should be considered

representative or typical only and should not be used for specification purposes.

Rate of Strength Build-Up

Aluminum, Overlap Shear (7 mil Bondline) (ASTM D 1002-72)

Bonds Tested at 73°F (23°C)

3M™Scotch-Weld™ Epoxy Adhesive DP460 Off-White

Time in Oven

Cure Temperature

73°F (23°C)

120°F1 (49°C)

140°F1 (60°C)

30 minutes

—

<50

3000/602

—

1300

4500/602

—

4300/602

—

2 hours

—

4400/602

4800

—

4800/602

—

400

—

1000

—

3500

—

4000/602

3M™Scotch-Weld™ Epoxy Adhesive DP460NS

Time in Oven

Cure Temperature

73°F (23°C)

120°F1 (49°C)

160°F1 (71°C)

15 minutes

—

4860

—

5250

—

2800

5300

2 hours

5050

5470

5400

5320

970

5570

5140

4500

—

5210

1This represents the oven temperature to which the bonds were subjected for the prescribed time. The average bondline temperature

during the cure time will be somewhat lower than the oven temperature.

2The value in the denominator is the expected minimum 73°F (23°C) T-peel strength (piw) measured after the indicated cure cycle.

NOTE: The data in this Technical Data Sheet were generated using the 3M™ EPX Applicator System equipped with an EPX static mixer,

according to manufacturer’s directions. Thorough hand-mixing will afford comparable results.

3M™ Scotch-Weld™ Epoxy Adhesives

DP460 Off-White • DP460NS

Typical

Adhesive

Performance

Characteristics

Note: The following technical information and data should be considered

representative or typical only and should not be used for specification purposes.

Substrates and Testing

A. Overlap Shear (ASTM D 1002-72)

Overlap shear (OLS) strengths were measured on 1 in. wide 1/2 in. overlap specimens. These

bonds were made individually using 1 in. x 4 in. pieces of substrate except for aluminum. Two

panels 0.063 in. thick, 4 in. x 7 in. of 2024T-3 clad aluminum were bonded and cut into 1 in.

wide samples after 24 hours. The thickness of the bondline was 0.005-0.008 in. All

strengths were measured at 73°F (23°C) except where noted.

The separation rate of the testing jaws was 0.1 in. per minute for metals, 2 in. per minute for

plastics and 20 in. per minute for rubbers. The thickness of the substrates were: steel, 0.060

in.; other metals, 0.05-0.064 in.; rubbers, 0.125 in.; plastics, 0.125 in.

B. T-peel (ASTM D 1876-61T)

T-peel strengths were measured on 1 in. wide bonds at 73°F (23°C). The testing jaw

separation rate was 20 inches per minute. The substrates were 0.032 in. thick.

C. Bell Peel (ASTM D 3167)

Bell peel strengths were measured on 1/2 in. wide bonds at the temperatures noted. The

testing jaw separation rate was 6 in. per minute. The bonds are made with 0.064 in. bonded to

0.025 in. thick adherends.

D. Cure Cycle

With the exception of Rate of Strength Build-Up Tests, all bonds, were cured 7 days at 73°F

(23°C) at 50% RH before testing or subjected to further conditioning or environmental

aging.

Aluminum, Overlap Shear, at Temperature (PSI)

3M™ Scotch-Weld™

Epoxy Adhesive

DP460 Off-White

3M™ Scotch-Weld™

Epoxy Adhesive

DP460NS

-67°F (-55°C)

4500

4900

73°F (23°C)

4500

4650

180°F (82°C) (15 min.)1

700

1360

(30 min.)1

1000

1810

(60 min.)1

1400

2630

(4 hr.)1

2500

2680

250°F (121°C) (15 min.)1

220

420

1Represents time in test chamber oven before test.

Metals, Overlap Shear, Tested @ 73°F (23°C) (PSI)

Aluminum Etched

4500

Oakite degreased

3200

2300

MEK/abrade/MEK

3500

2670

Cold Rolled Steel Oakite degreased

3500

—

MEK/abrade/MEK

2800

3600

Copper MEK/abrade/MEK

4000

4400

Brass MEK/abrade/MEK

—

3400

CDA 260

4000

—

Cartridge

4200

—

Stainless Steel MEK/abrade/MEK

4000

2400

Galvanized Steel - Oakite degreased

2000

2480

Hot dipped

Electrodeposited

2100

3000

3M™ Scotch-Weld™ Epoxy Adhesives

DP460 Off-White • DP460NS

Typical

Adhesive

Performance

Characteristics

(continued)

Note: The following technical information and data should be considered

representative or typical only and should not be used for specification purposes.

Substrates and Testing

Aluminum, T-Peel (PIW), at Temperature

Aluminum, etched (17-20 mil bondline)

Metals, T-Peel, Tested @ 73°F (23°C) (PIW)

Aluminum Bell Peel (PIW), at Temperature (ASTM D 3167)

Other Substrates, Overlap Shear Tested @ 73°F (23°C)

1Isopropyl Alcohol Wipe. See Surface Preparation Section D for additional information.

2Isopropyl Alcohol/Abrade/Isopropyl Alcohol: See Surface Preparation Section E for additional

information.

3Substrate failure

Aluminum, etched 17-20 mil bondline

5-8 mil bondline

not tested

Cold Rolled Steel 17-20 mil bondline

Oakite degreased

MEK/abrade/MEK

not tested

Temperature

3M™ Scotch-Weld™

Epoxy Adhesive DP460NS

-67°F (-55°C)

73°F (23°C)

180°F (82°C)

3M™ Scotch-Weld™

Epoxy Adhesive

DP460 Off-White

3M™ Scotch-Weld™

Epoxy Adhesive

DP460NS

-67°F (-55°C)

5-10

3-5

73°F (23°C)

180°F (82°C)

3-5

Substrate

Surf. Prep.1

3M™ Scotch-Weld™ Epoxy Adhesive

DP460 Off-White DP460NS

Surf. Prep.2

3M™ Scotch-Weld™ Epoxy Adhesive

DP460 Off-White DP460NS

ABS

300

345

575

572

PVC

500

8153

350

3133

Polycarbonate

400

380

500

390

Polyacrylic

220

210

330

270

Polystryene

450

320

4753

490

FRP

800

570

10003

13793

Phenolic

14003

12103

14003

12313

SBR/Steel

1503

130

1403

2393

Neoprene/Steel

100

1203

1143

3M™ Scotch-Weld™ Epoxy Adhesives

DP460 Off-White • DP460NS

Typical

Adhesive

Performance

Characteristics

(continued)

Note: The following technical information and data should be considered

representative or typical only and should not be used for specification purposes.

Substrates and Testing (continued)

Environmental Resistance, Aluminum (Etched)

Measured by Overlap Shear Tested @ 73°F (23°C) (PSI)1 (ASTM D 1002-72)

Environment

Condition

3M™ Scotch-Weld™ Epoxy Adhesive

DP460 Off-White

DP460NS

DP460 Off-White

DP460NS

73°F (23°C)/50% RH

30 d2

5200

5460

Distilled Water

30 d, i3

5100

4550

Water Vapor

120°F (49°C)/100% RH, 30 d

200°F (93°C)/100% RH, 14 d

4500

3100

3920

3370

Antifreeze/H

O (50/50)

180°F (82°C), 30 d, i

5000

4400

Isopropyl Alcohol

73°F (23°C), 30 d, i

5700

5320

Methyl Ethyl Ketone

73°F (23°C), 30 d, i

4200

4000

Salt Spray (5%)

95°F (35°C), 30 d

5100

5200

Skydrol LD-4

150°F (66°C), 30 d, i

3700

5250

1Data reported are actual values from the lots tested and may be higher than values published elsewhere in this Technical Data Sheet.

d = days

i = immersion

Environmental Resistance, Galvanized Steels1

Measured by Overlap Shear Tested @ 73°F (23°C) (PSI)2 (ASTM D 1002-72)

Environment

Condition

Hot Dipped

3M™ Scotch-Weld™

Epoxy

Adhesive

DP460 DP460

Off-White NS

Electrodeposited

3M™ Scotch-Weld™

Epoxy

Adhesive

DP460 DP460

Off-White NS

73°F (23°C)/50% RH

30 d3

2200

not tested

2300

not tested

Distilled Water

30 d, i4

2300

not tested

2300

not tested

Water Vapor

120°F (49°C)/100% RH, 30 d

200°F (93°C)/100% RH, 14 d

1900

1500

not tested

2000

1000

not tested

Antifreeze/H2O

(50/50)

180°F (82°C), 30 d, i

2000

not tested

1950

not tested

Isopropyl Alcohol

73°F (23°C), 30 d, i

2000

not tested

2200

not tested

Methyl Ethyl Ketone

73°F (23°C), 30 d, i

2000

not tested

2200

not tested

Trichloroethane

73°F (23°C), 30 d, i

2300

not tested

2300

not tested

Salt Spray (5%)

95°F (35°C), 30d

1900

not tested

1500

not tested

1Hot dipped or electrodeposited. Galvanized steels may afford a wide spectrum of performance due to the diversity of surfaces

available. The user should test to determine specific performance.

2Data reported are actual values from the lots tested and may be higher than values published elsewhere in this Technical Data Sheet.

3d = days

i = immersion

3M™ Scotch-Weld™ Epoxy Adhesives

DP460 Off-White • DP460NS

3M™ EPX

Pneumatic

Applicator

Delivery Rates

200 ml Applicator – Maximum Pressure 58 psi

Adhesive*

6mm Nozzle

gms/minute

10mm Nozzle

gms/minute

3M™ Scotch-Weld™ Epoxy Adhesive DP460 Off-White

31.1

132.0

*Tests were run at a temperature of 70°F ± 2°F (21°C ± 1°C) and at maximum applicator pressure.

Handling/

Application

Information

Directions for Use

3M™ Scotch-Weld™ Epoxy Adhesives DP460 Off-White and DP460 NS are

supplied in dual syringe plastic duo-pak cartridges as part of the 3M™ EPX

Applicator System. The duo-pak cartridges are supplied in 37 ml, 200 ml and 400

ml configurations. To use the 37 ml cartridge simply insert the duo-pak cartridge

into the EPX applicator and start the plunger into the cylinders using light pressure

on the trigger. Next, remove the duo-pak cartridge cap and expel a small amount of

adhesive to be sure both sides of the duo-pak cartridge are flowing evenly and

freely. If simultaneous mixing of Part A and Part B is desired, attach the EPX mixing

nozzle to the duo-pak cartridge and begin dispensing the adhesive.

With the 200 ml and 400 ml cartridges, the nozzle must be attached before

dispensing any material to prevent unmixed adhesive from getting into the

applicator cartridge holder. A small quantity of material should be discarded until

uniform color, consistency of product and even flow is evident.

When mixing Part A and Part B manually, the components must be mixed in the

ratio indicated in the typical uncured properties section. Complete mixing of the

two components is required to obtain optimum properties.

Two-part mixing/proportioning/dispensing equipment is available for intermittent

or production line use. These systems are ideal for line uses because of their

variable shot size and flow rate characteristics and are adaptable to most

applications.

3M™ Scotch-Weld™ Epoxy Adhesives

DP460 Off-White • DP460NS

Surface Preparation The following surface preparations were used for substrates described in this

Technical Data Sheet.

A. Aluminum Etch

Optimized FPL Etch - 3M (test method C-2803)

1. Alkaline degrease – Oakite 164 solution (9-11 oz./gallon water) at 190°F ±

10°F (88°C ± 5°C) for 10-20 minutes. Rinse immediately in large quantities

of cold running water (3M test method C-2802).

2. Optimized FPL Etch Solution (1 liter):

Material Amount

Distilled Water 700 ml plus balance of liter (see below)

Sodium Dichromate 28 to 67.3 grams

Sulfuric Acid 287.9 to 310.0 grams

Aluminum Chips 1.5 grams/liter of mixed solution

To prepare 1 liter of this solution, dissolve sodium dichromate in 700 ml of

distilled water. Add sulfuric acid and mix well. Add additional distilled water

to fill to 1 liter. Heat mixed solution to 66 to 71°C (150 to 160°F). Dissolve

1.5 grams of 2024 bare aluminum chips per liter of mixed solution. Gentle

agitation will help aluminum dissolve in about 24 hours.

To FPL etch panels, place them in the above solution at 150 to 160°F (66 to

71°C) for 12 to 15 minutes.

Note: Review and follow precautionary information provided by

chemical suppliers prior to preparation of this etch solution.

3. Rinse immediately in large quantities of clear running tap water.

4. Dry – air dry approximately 15 minutes followed by force dry at 140°F

(60°C) maximum for 10 minutes (minimum).

5. Both surface structure and chemistry play a significant role in determining

the strength and permanence of bonded structures. It is therefore advisable

to bond or prime freshly primed clean surfaces as soon as possible after

surface preparation in order to avoid contamination and/or mechanical

damage. Please contact your 3M sales representative for primer

recommendations.

B. Oakite Degrease

Oakite 164 solutions (9-11 oz./gallon of water) at 190°F ± 10°F (88°C ± 5°C) for 2

minutes. Rinse immediately in large quantities of cold running water.

C. MEK/Abrade/MEK

Wipe surface with a methyl ethyl ketone (MEK) soaked swab, abrade and wipe

with a MEK soaked swab.* Allow solvent to evaporate before applying adhesive.

D. Isopropyl Alcohol Wipe

Wipe surface with an isopropyl alcohol soaked swab.* Allow solvent to evaporate

before applying adhesive.

E. Isopropyl Alcohol/Abrade/Isopropyl Alcohol

Wipe surface with an isopropyl alcohol soaked swab, abrade using clean fine grit

abrasives, and wipe with an isopropyl alcohol soaked swab.* Then allow solvent

to evaporate before applying adhesive.

*Note: When using solvents, extinguish all ignition sources, including pilot lights,

and follow the manufacturer’s precautions and directions for use.

3M™ Scotch-Weld™ Epoxy Adhesives

DP460 Off-White • DP460NS

Storage Store products at 60-80°F (15-27°C) for maximum shelf life.

Shelf Life These products have a shelf life of 24 months from date of manufacture in original containers

at room temperature

Technical

Information

The technical information, guidance, and other statements contained in this document or otherwise

provided by 3M are based upon records, tests, or experience that 3M believes to be reliable, but the

accuracy, completeness, and representative nature of such information is not guaranteed. Such information

is intended for people with knowledge and technical skills sufficient to assess and apply their own informed

judgment to the information. No license under any 3M or third party intellectual property rights is granted

or implied with this information.

Product Selection

and Use

Many factors beyond 3M’s control and uniquely within user’s knowledge and control can affect the use

and performance of a 3M product in a particular application. As a result, customer is solely responsible

for evaluating the product and determining whether it is appropriate and suitable for customer’s

application, including conducting a workplace hazard assessment and reviewing all applicable regulations

and standards (e.g., OSHA, ANSI, etc.). Failure to properly evaluate, select, and use a 3M product and

appropriate safety products, or to meet all applicable safety regulations, may result in injury, sickness,

death, and/or harm to property.

Warranty,

Limited Remedy,

and Disclaimer

Unless a different warranty is specifically stated on the applicable 3M product packaging or product

literature (in which case such warranty governs), 3M warrants that each 3M product meets the

applicable 3M product specification at the time 3M ships the product. 3M MAKES NO OTHER

WARRANTIES OR CONDITIONS, EXPRESS OR IMPLIED, INCLUDING, BUT NOT LIMITED TO, ANY

IMPLIED WARRANTY OR CONDITION OF MERCHANTABILITY, FITNESS FOR A PARTICULAR

PURPOSE, OR ARISING OUT OF A COURSE OF DEALING, CUSTOM, OR USAGE OF TRADE. If a 3M

product does not conform to this warranty, then the sole and exclusive remedy is, at 3M’s option,

replacement of the 3M product or refund of the purchase price.

Limitation of Liability Except for the limited remedy stated above, and except to the extent prohibited by law, 3M will not be

liable for any loss or damage arising from or related to the 3M product, whether direct, indirect, special,

incidental, or consequential (including, but not limited to, lost profits or business opportunity),

regardless of the legal or equitable theory asserted, including, but not limited to, warranty, contract,

negligence, or strict liability.

ISO 9001

This Industrial Adhesives and Tapes Division product was manufactured under a 3M quality system registered to ISO 9001 standards.

Industrial Adhesives and Tapes Division

3M Center, Building 225-3S-06

St. Paul, MN 55144-100

800-362-3550 977-369-2923 ( Fax)

www.3M.com/structuraladhesives

3M and Scotch-Weld are trademarks of

3M Company.